Using a combination of transient plane source (TPS) technique and slug calorimetry, 4 commercially available fire resistive materials (FRMs) are studied from room temperature to 1000°C. The materials studied in this report are two gypsum-based and two calcium-silicate based materials. These materials are heterogeneous and thus when heated to elevated temperatures, the microstructure of the materials may be compromised and various reactions and phase changes may take place over the course ...
Thermal interface resistance results from small gaps and surface geometry mismatches between two materials that make up a composite. Thermal interface resistance is present in most any material that is comprised of two or more components. In the field of thermal interface materials, the majority of novel materials are composites, and thus are subject to thermal interface resistance and thermal boundary resistance (thermal discontinuity at a perfectly bonded interface of ...
In this article, the authors present a novel method for the synthesis of graphene layers that can be used in advanced electronic devices, among other applications. The preparation method involves the use of a high-pressure high-temperature process where the pressure and temperature are closely monitored in order to preferentially prepare graphene layers. The quality of the material synthesized is much better than previously reported, and the size of the layers ...
A series of compacted Bi0.5Sb1.5Te3 nanoplatelets are synthesized using hydrothermal methods, followed by cold pressing and sintering at temperatures between 300°C and 380°C. A variety of thermal, mechanical and electrical analyses are then performed on the synthesized nanoplatelets including: TPS technique for thermal conductivity, SEM/TEM/AFM to elucidate the mechanical and physical properties of the nanoplatelets, and the Oxford closed cycle cooler cryostat for measurement of electrical ...
Using a three-roll mill process, graphite nanoplatelets (GNPs) were dispersed in a silicone polymer for application as a thermal interface material. Through the use of electron microscopy and XRD, the researchers were able to determine that the GNPs dispersed better when using the three-roll milling process as compared to previously used methods. GNPs were mixed with the silicone polymer in wt.% up to 25, with the highest wt.% yielding the highest ...
