The authors prepared PMMA/clay composites by the in situ bulk polymerization method. The prepared composites were characterized by FT-IR, WAXRD, SEM, TEM, DMA and the transient plane source (TPS) technique to measure thermal conductivity. Not only were the thermal properties of the composites studied, but physical and chemical properties as well....
Sebacic acid (SA) can be absorbed into the pores of expanded graphite (EG) to form a SA/EG composite phase change material (PCM). There is no chemical interaction between the SA and EG, they are merely integrated. The optimal amount of SA was found to be 85 wt.% of the total mixture. The 85 wt.% composite had a phase change temperature of ~ 128°C, with a latent heat of ~ 187 J/g. The thermal ...
Microencapsulated phase change materials (MPCMs) are excellent materials for the storage of thermal energy, and through their dispersal into a carrier fluid, microencapsulated phase change slurries (MPCS) can be prepared. These slurries exhibit both excellent thermal energy storage and heat transfer properties. A series of MPCS were prepared for this research and subsequently tested for thermal conductivity and specific heat. Other methods of quantification include DSC, TGA, rheometry, and infrared ...
The main objective of this research project was to create a material with a very low thermal conductivity at high temperatures, for the conservation of energy in high temperature systems. To accomplish this goal, the researchers incorporated carbon nanofibers into the mesoporous network of monolithic aerogels, with up to a 20 wt.% through an accelerated-gelation sol-gel process. The synthesis process also involved the use of supercritical drying of the aerogels to ...
A series of melamine-formaldehyde microcapsules were synthesized using an in-situ polymerization and subsequently characterized for their thermal and structural properties. SEM and FT-IR were used to investigate the structural properties and DSC and TGA were used to investigate the thermal properties. The authors concluded that the thermo-physical properties of the microcapsules were related to the synthesis conditions and the core content of the capsules....