A series of compacted Bi0.5Sb1.5Te3 nanoplatelets are synthesized using hydrothermal methods, followed by cold pressing and sintering at temperatures between 300°C and 380°C. A variety of thermal, mechanical and electrical analyses are then performed on the synthesized nanoplatelets including: TPS technique for thermal conductivity, SEM/TEM/AFM to elucidate the mechanical and physical properties of the nanoplatelets, and the Oxford closed cycle cooler cryostat for measurement of electrical ...
Using a three-roll mill process, graphite nanoplatelets (GNPs) were dispersed in a silicone polymer for application as a thermal interface material. Through the use of electron microscopy and XRD, the researchers were able to determine that the GNPs dispersed better when using the three-roll milling process as compared to previously used methods. GNPs were mixed with the silicone polymer in wt.% up to 25, with the highest wt.% yielding the highest ...
In order to prepare more thermally resistant materials for use as thermal barrier coatings, the authors performed experiments on yttrium stabilized-zirconia (7YSZ) in order to investigate sintering resistance and phase stability at high temperatures. It was theorized that the main factor that affected the sintering resistance and phase stability at high temperatures was the concentration of impurities (Al2O3 and Si2O) present in the 7YSZ. Therefore in this report ...
Measurements were carried out to determine the electrical resistivity, thermal conductivity and Seebeck coefficients of a series of Fe-doped misfit-layered oxides (Ca3Co(4-x)Fe(x)O(9+delta) (x=0, 0.05, 0.1, and 0.2)). The thermal conductivity experiments were carried out using a Thermal Constants Analyzer via the TPS technique. XRD was also used to characterize the Fe-doped oxides. Overall, the transport properties of the Fe-doped oxides were studied and it was found that ...
Yttria-stabilized zirconia (YSZ) was synthesized by the spark plasma sintering process to generate pore-free, homogenous bulk samples that were then tested for thermal conductivity, which was measured by two separate methods: TPS and LFT. The TPS method was found to be better for measuring of thermal conductivity in this specific case. Using the phonon-hopping model (PHM) the authors were able to determine how grain boundaries of the bulk samples affected ...
