Using a combination of transient plane source (TPS) technique and slug calorimetry, 4 commercially available fire resistive materials (FRMs) are studied from room temperature to 1000°C. The materials studied in this report are two gypsum-based and two calcium-silicate based materials. These materials are heterogeneous and thus when heated to elevated temperatures, the microstructure of the materials may be compromised and various reactions and phase changes may take place over the course ...
The authors used the transient plane source technique for measuring the thermal conductivity, diffusivity and specific heat of highly porous materials. This paper helped to demonstrate that the newly developed TPS technique wasn't just for the measurement of isotropic bulk materials. Different samples of wood composites were analyzed. Once measurements were obtained using the TPS method, they were compared to results obtained theoretically using Verma's model for prediction of thermal ...
The authors highlight different methods of studying the purity, composition, and structural changes of polymeric and glass materials. These methods include the use of differential scanning calorimetry (DSC) and the transient plane source (TPS) technique. The quality of the TPS Technique is outlined and the authors praise the high quality of the machine. In addition to this, thermal analysis is carried out on some polymeric composites (cis-polyisoprene (CPI)/trans-polyisoprene (TPI) ...
The authors look into problems with accurately measuring thermal conductivity of liquid samples. Among these problems is the onset of natural convection during the measurement of thermal properties, which may lead to skewed values reported after characterization. The effect of natural convection is analyzed numerically for the transient plane source method in order to determine at what time during an analysis the convection causes incorrect output data. The effect of ...
The researchers proposed a method used to measure the thermal conductivity and heat capacity of low thermal conductivity materials with accuracy better than 10%. DSC was also used to determine thermal contact between the sample and the DSC furnace....
