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Ambient pressure dried hydrophobic silica aerogel monoliths were prepared via simultaneous solvent exchange and surface modification in order to minimize volume shrinkage and density. At room temperature, the obtained silica aerogels had a low density of 0.096 g/cm3, a high surface area and hydrophobicity, and a low thermal conductivity of 0.0217 W/m·K. The effect of heating on these properties was also determined. After the aerogel had been heated to 300...
Ultralow density silica aerogels were formulated by sol-gel process using tetramethyl orthosilicate as the precursor. A supercritical drying step was performed using acetonitrile solvent extraction. These aerogels were found to have a high specific surface area (~812m2/g) and they were found to be excellent thermal insulators with thermal conductivities ranging from 0.024 to 0.043 W/m K at temperatures up to 400oC....
In this study, ultralow density silica aerogels were synthesized and their thermal conductivities were tested to determine how supercritical drying affected the samples. A thermal analyzer measured the thermal conductivity of the silica aerogels using the transient plane source (TPS) method which determined that the thermal conductivity of silica aerogels increased with temperature....
